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Information card for entry 4034618
Preview
Coordinates | 4034618.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H20 F O2 P |
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Calculated formula | C27 H20 F O2 P |
Title of publication | Photoredox/Cobalt-Catalyzed Phosphinyloxy Radical Addition/Cyclization Cascade: Synthesis of Phosphaisocoumarins. |
Authors of publication | Qiao, Ming-Ming; Liu, Yi-Yin; Yao, Sheng; Ma, Tian-Cong; Tang, Zi-Long; Shi, De-Qing; Xiao, Wen-Jing |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2019 |
Journal volume | 84 |
Journal issue | 11 |
Pages of publication | 6798 - 6806 |
a | 9.395 ± 0.003 Å |
b | 10.61 ± 0.003 Å |
c | 11.09 ± 0.004 Å |
α | 75.545 ± 0.006° |
β | 84.22 ± 0.007° |
γ | 76.423 ± 0.007° |
Cell volume | 1039.5 ± 0.6 Å3 |
Cell temperature | 273 ± 2 K |
Ambient diffraction temperature | 273.15 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.083 |
Residual factor for significantly intense reflections | 0.0454 |
Weighted residual factors for significantly intense reflections | 0.0943 |
Weighted residual factors for all reflections included in the refinement | 0.1166 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4034618.html
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Users of the data should acknowledge the original authors of the
structural data.