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Information card for entry 4035444
Preview
Coordinates | 4035444.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H54 O6 Si2 |
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Calculated formula | C30 H54 O6 Si2 |
SMILES | [Si](O[C@]12C(=O)O[C@]([C@@H]2CC[C@@H]2[C@@](OC(=O)C2)(C1)CCC(=C)C)(CO[Si](C(C)(C)C)(C)C)C)(CC)(CC)CC |
Title of publication | Asymmetric Total Synthesis of Lancifodilactone G Acetate. 2. Final Phase and Completion of the Total Synthesis. |
Authors of publication | Wang, Kuang-Yu; Liu, Dong-Dong; Sun, Tian-Wen; Lu, Yong; Zhang, Su-Lei; Li, Yuan-He; Han, Yi-Xin; Liu, Hao-Yuan; Peng, Cheng; Wang, Qin-Yang; Chen, Jia-Hua; Yang, Zhen |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2018 |
Journal volume | 83 |
Journal issue | 13 |
Pages of publication | 6907 - 6923 |
a | 9.47108 ± 0.00012 Å |
b | 11.24253 ± 0.00017 Å |
c | 30.714 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3270.39 ± 0.08 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0338 |
Residual factor for significantly intense reflections | 0.0336 |
Weighted residual factors for significantly intense reflections | 0.0884 |
Weighted residual factors for all reflections included in the refinement | 0.0885 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.086 |
Diffraction radiation wavelength | 1.5418 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4035444.html
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Users of the data should acknowledge the original authors of the
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