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Information card for entry 4035503
Preview
Coordinates | 4035503.cif |
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Original paper (by DOI) | HTML |
Formula | C22 H21.25 N O5.25 |
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Calculated formula | C22 H21.25 N O5.25 |
Title of publication | Palladium(II)-Catalyzed Mono- and Bis-alkenylation of N-Acetyl-2-aminobiaryls through Regioselective C-H Bond Activation. |
Authors of publication | Annamalai, Pratheepkumar; Hsu, Kou-Chi; Raju, Selvam; Hsiao, Huan-Chang; Chou, Chih-Wei; Lin, Gu-Ying; Hsieh, Cheng-Ming; Chen, Pei-Ling; Liu, Yi-Hung; Chuang, Shih-Ching |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2018 |
Journal volume | 83 |
Journal issue | 7 |
Pages of publication | 3840 - 3856 |
a | 16.2526 ± 0.0004 Å |
b | 16.9979 ± 0.0005 Å |
c | 14.2159 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3927.3 ± 0.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 4 |
Space group number | 60 |
Hermann-Mauguin space group symbol | P b c n |
Hall space group symbol | -P 2n 2ab |
Residual factor for all reflections | 0.09 |
Residual factor for significantly intense reflections | 0.0539 |
Weighted residual factors for significantly intense reflections | 0.1471 |
Weighted residual factors for all reflections included in the refinement | 0.1808 |
Goodness-of-fit parameter for all reflections included in the refinement | 1 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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