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Information card for entry 4036464
Preview
Coordinates | 4036464.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H23 N O4 |
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Calculated formula | C24 H23 N O4 |
SMILES | Nc1ccccc1C(=O)C(c1ccc(cc1)OC)CC(=O)c1ccc(cc1)OC |
Title of publication | 2-Oxindole Acts as a Synthon of 2-Aminobenzoyl Anion in the K2CO3-Catalyzed Reaction with Enones: Preparation of 1,4-Diketones Bearing an Amino Group and Their Further Transformations. |
Authors of publication | Miao, Chun-Bao; Zeng, Yu-Mei; Shi, Tong; Liu, Rui; Wei, Peng-Fei; Sun, Xiao-Qiang; Yang, Hai-Tao |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2016 |
Journal volume | 81 |
Journal issue | 1 |
Pages of publication | 43 - 50 |
a | 8.024 ± 0.002 Å |
b | 9.535 ± 0.003 Å |
c | 13.836 ± 0.004 Å |
α | 87.961 ± 0.006° |
β | 81.861 ± 0.006° |
γ | 69.892 ± 0.006° |
Cell volume | 983.9 ± 0.5 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0603 |
Residual factor for significantly intense reflections | 0.0499 |
Weighted residual factors for significantly intense reflections | 0.1349 |
Weighted residual factors for all reflections included in the refinement | 0.1414 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.088 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4036464.html
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