Information card for entry 4036997

Structure parameters

• Formula: C24 H26 Cl2 N Rh
• Calculated formula: C24 H26 Cl2 N Rh
• Title of publication: Rhodium-Catalyzed NH-Indole-Directed C-H Carbonylation with Carbon Monoxide: Synthesis of 6H-Isoindolo[2,1-a]indol-6-ones.
• Authors of publication: Huang, Qiufeng; Han, Qingshuai; Fu, Shurong; Yao, Zizhu; Su, Lv; Zhang, Xiaofeng; Lin, Shen; Xiang, Shengchang
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2016
• Journal volume: 81
• Journal issue: 24
• Pages of publication: 12135 - 12142
• a: 8.7872 ± 0.0005 Å
• b: 18.8893 ± 0.0011 Å
• c: 26.3974 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4381.5 ± 0.4 ų
• Cell temperature: 291.98 ± 0.1 K
• Ambient diffraction temperature: 291.98 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.15
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for significantly intense reflections: 0.0822
• Weighted residual factors for all reflections included in the refinement: 0.1098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No