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Information card for entry 4037003
Preview
Coordinates | 4037003.cif |
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Original paper (by DOI) | HTML |
Formula | C30 H41 N3 O7 S |
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Calculated formula | C30 H41 N3 O7 S |
Title of publication | Asymmetric Michael Addition Induced by (R)-tert-Butanesulfinamide and Syntheses of Chiral Pyrazolidinone Derivatives. |
Authors of publication | Huang, Hong-Xiu; Wang, Hui-Jing; Tan, Ling; Wang, Shu-Qing; Tang, Pei; Song, Hao; Liu, Xiao-Yu; Zhang, Dan; Qin, Yong |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2016 |
Journal volume | 81 |
Journal issue | 21 |
Pages of publication | 10506 - 10516 |
a | 8.3265 ± 0.0002 Å |
b | 10.1974 ± 0.0003 Å |
c | 38.2435 ± 0.0016 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3247.2 ± 0.18 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293.15 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0897 |
Residual factor for significantly intense reflections | 0.0667 |
Weighted residual factors for significantly intense reflections | 0.1858 |
Weighted residual factors for all reflections included in the refinement | 0.2072 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4037003.html
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