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Information card for entry 4037065
Preview
Coordinates | 4037065.cif |
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Original paper (by DOI) | HTML |
Formula | C20 H27 N3 O2 |
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Calculated formula | C20 H27 N3 O2 |
Title of publication | A Formal Total Synthesis of (±)-Kopsihainanine A Using a Raney-Cobalt Mediated Reductive Cyclization Route to Polyhydroquinolines. |
Authors of publication | Tan, Shen H.; Banwell, Martin G.; Willis, Anthony C. |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2016 |
Journal volume | 81 |
Journal issue | 17 |
Pages of publication | 8022 - 8028 |
a | 8.3982 ± 0.0001 Å |
b | 10.5143 ± 0.0002 Å |
c | 20.8016 ± 0.0004 Å |
α | 90° |
β | 94.8955 ± 0.001° |
γ | 90° |
Cell volume | 1830.11 ± 0.05 Å3 |
Cell temperature | 200 K |
Ambient diffraction temperature | 200 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0554 |
Residual factor for significantly intense reflections | 0.0397 |
Weighted residual factors for all reflections | 0.1028 |
Weighted residual factors for significantly intense reflections | 0.0955 |
Weighted residual factors for all reflections included in the refinement | 0.1028 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.9581 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4037065.html
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structural data.