Information card for entry 4037079

Structure parameters

• Formula: C23 H22 N2 O4
• Calculated formula: C23 H22 N2 O4
• Title of publication: A Raney Cobalt Mediated Reductive Cyclization Route to the Uleine Alkaloid Gilbertine.
• Authors of publication: Tang, Fei; Banwell, Martin G.; Willis, Anthony C.
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2016
• Journal volume: 81
• Journal issue: 21
• Pages of publication: 10551 - 10557
• a: 5.856 ± 0.0002 Å
• b: 11.9176 ± 0.0004 Å
• c: 15.3239 ± 0.0007 Å
• α: 109.83 ± 0.004°
• β: 97.254 ± 0.003°
• γ: 99.9 ± 0.003°
• Cell volume: 971.19 ± 0.07 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0466
• Residual factor for significantly intense reflections: 0.0413
• Weighted residual factors for all reflections: 0.1048
• Weighted residual factors for significantly intense reflections: 0.1007
• Weighted residual factors for all reflections included in the refinement: 0.1048
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9915
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No