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Information card for entry 4037284
Preview
Coordinates | 4037284.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C86 H96 N8 O24.21 P2 |
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Calculated formula | C86 H96 N8 O24.205 P2 |
Title of publication | Scalable Synthesis of Enantiopure Bis-3,4-diazaphospholane Ligands for Asymmetric Catalysis. |
Authors of publication | Jones, Bradley R.; Abrams, M. Leigh; Landis, Clark R.; May, Scott A.; Campbell, Alison N.; Martinelli, Joseph R.; Calvin, Joel R. |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2016 |
Journal volume | 81 |
Journal issue | 23 |
Pages of publication | 11965 - 11970 |
a | 19.2424 ± 0.0006 Å |
b | 19.606 ± 0.0007 Å |
c | 50.4378 ± 0.0016 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 19028.5 ± 1.1 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1688 |
Residual factor for significantly intense reflections | 0.1501 |
Weighted residual factors for significantly intense reflections | 0.4166 |
Weighted residual factors for all reflections included in the refinement | 0.4728 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.01 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4037284.html
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structural data.