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Information card for entry 4037444
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Coordinates | 4037444.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H28 F7 N O5 |
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Calculated formula | C25 H28 F7 N O5 |
Title of publication | Diastereoselective Trifluoroacetylation of Highly Substituted Pyrrolidines by a Dakin-West Process. |
Authors of publication | Baumann, Marcus; Baxendale, Ian R. |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2016 |
Journal volume | 81 |
Journal issue | 23 |
Pages of publication | 11898 - 11908 |
a | 9.3392 ± 0.0006 Å |
b | 12.0373 ± 0.0008 Å |
c | 25.2796 ± 0.0017 Å |
α | 101.028 ± 0.003° |
β | 92.592 ± 0.003° |
γ | 111.947 ± 0.003° |
Cell volume | 2565.9 ± 0.3 Å3 |
Cell temperature | 120 K |
Ambient diffraction temperature | 120 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1057 |
Residual factor for significantly intense reflections | 0.0855 |
Weighted residual factors for significantly intense reflections | 0.2158 |
Weighted residual factors for all reflections included in the refinement | 0.2254 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.086 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4037444.html
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Users of the data should acknowledge the original authors of the
structural data.