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Information card for entry 4037603
Preview
Coordinates | 4037603.cif |
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Original paper (by DOI) | HTML |
Chemical name | '5,5'-Dibromo-3,3'-diiodo-[4,4']bipyridinyl' |
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Formula | C10 H4 Br2 I2 N2 |
Calculated formula | C10 H4 Br2 I2 N2 |
Title of publication | Synthesis, resolution, and absolute configuration of chiral 4,4'-bipyridines. |
Authors of publication | Mamane, Victor; Aubert, Emmanuel; Peluso, Paola; Cossu, Sergio |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2012 |
Journal volume | 77 |
Journal issue | 6 |
Pages of publication | 2579 - 2583 |
a | 8.078 ± 0.0001 Å |
b | 11.2993 ± 0.0001 Å |
c | 15.5039 ± 0.0002 Å |
α | 102.689 ± 0.001° |
β | 98.153 ± 0.001° |
γ | 90.893 ± 0.001° |
Cell volume | 1365.01 ± 0.03 Å3 |
Cell temperature | 110 ± 2 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 5 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0361 |
Residual factor for significantly intense reflections | 0.0317 |
Weighted residual factors for significantly intense reflections | 0.0685 |
Weighted residual factors for all reflections included in the refinement | 0.0707 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4037603.html
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