Information card for entry 4038199
Formula |
C18 H12 N O3 |
Calculated formula |
C18 H12 N O3 |
Title of publication |
N-Acyl-Glutarimides: Effect of Glutarimide Ring on the Structures of Fully Perpendicular Twisted Amides and N-C Bond Cross-Coupling. |
Authors of publication |
Rahman, Md Mahbubur; Liu, Chengwei; Bisz, Elwira; Dziuk, Błażej; Lalancette, Roger A.; Wang, Qi; Chen, Hao; Szostak, Roman; Szostak, Michal |
Journal of publication |
The Journal of organic chemistry |
Year of publication |
2020 |
a |
8.4816 ± 0.0007 Å |
b |
8.7359 ± 0.0011 Å |
c |
20.784 ± 0.002 Å |
α |
90° |
β |
95.956 ± 0.01° |
γ |
90° |
Cell volume |
1531.7 ± 0.3 Å3 |
Cell temperature |
293 ± 2 K |
Ambient diffraction temperature |
293 ± 2 K |
Number of distinct elements |
4 |
Space group number |
14 |
Hermann-Mauguin space group symbol |
P 1 21/n 1 |
Hall space group symbol |
-P 2yn |
Residual factor for all reflections |
0.17 |
Residual factor for significantly intense reflections |
0.0638 |
Weighted residual factors for significantly intense reflections |
0.1705 |
Weighted residual factors for all reflections included in the refinement |
0.2226 |
Goodness-of-fit parameter for all reflections included in the refinement |
0.936 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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https://www.crystallography.net/4038199.html