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Information card for entry 4038301
Preview
Coordinates | 4038301.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | 8-chloro-6,6-dimethyl-5-phenyl-6H-indeno[2,1-b]phosphindole 5-oxide |
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Formula | C23 H18 Cl O P |
Calculated formula | C23 H18 Cl O P |
Title of publication | Azobisisobutyronitrile-Initiated Oxidative C-H Functionalization of Simple Alcohols with Diaryl(arylethynyl)phosphine Oxides: A Metal-Free Approach toward Hydroxymethyl Benzo[<i>b</i>]phosphole Oxides and 6<i>H</i>-Indeno[2,1-<i>b</i>]phosphindole 5-Oxide Derivatives. |
Authors of publication | Guo, Jiami; Mao, Chenlu; Deng, Bin; Ye, Liyi; Yin, Yingwu; Gao, Yuxing; Tu, Song |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2020 |
a | 7.6089 ± 0.0002 Å |
b | 14.041 ± 0.0003 Å |
c | 17.1323 ± 0.0004 Å |
α | 90° |
β | 93.246 ± 0.002° |
γ | 90° |
Cell volume | 1827.42 ± 0.08 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0478 |
Residual factor for significantly intense reflections | 0.0408 |
Weighted residual factors for significantly intense reflections | 0.1077 |
Weighted residual factors for all reflections included in the refinement | 0.1158 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4038301.html
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