Information card for entry 4038317
Formula |
C33 H37 N3 O2 |
Calculated formula |
C33 H37 N3 O2 |
Title of publication |
Palladium-Catalyzed Cycloaddition of Alkynylimines, Double Isocyanides, and H2O/KOAc. |
Authors of publication |
Chen, Dianpeng; Yang, Min; Li, Jianming; Cui, Peiying; Su, Lei; Shan, Yingying; You, Jinmao; Rojsitthisak, Pornchai; Liu, Jin-Biao; Qiu, Guanyinsheng |
Journal of publication |
The Journal of organic chemistry |
Year of publication |
2020 |
a |
11.5651 ± 0.0006 Å |
b |
20.5701 ± 0.0011 Å |
c |
12.4399 ± 0.0007 Å |
α |
90° |
β |
95.914 ± 0.005° |
γ |
90° |
Cell volume |
2943.6 ± 0.3 Å3 |
Cell temperature |
295 ± 2 K |
Ambient diffraction temperature |
295 ± 2 K |
Number of distinct elements |
4 |
Space group number |
14 |
Hermann-Mauguin space group symbol |
P 1 21/c 1 |
Hall space group symbol |
-P 2ybc |
Residual factor for all reflections |
0.0894 |
Residual factor for significantly intense reflections |
0.0579 |
Weighted residual factors for significantly intense reflections |
0.1475 |
Weighted residual factors for all reflections included in the refinement |
0.1681 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.033 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/4038317.html