Information card for entry 4038379

Structure parameters

• Formula: C19 H22 O6
• Calculated formula: C19 H22 O6
• Title of publication: CuBr₂-Mediated One-Pot Synthesis of Sulfonyl 9-Fluorenylidenes.
• Authors of publication: Chang, Meng-Yang; Tsai, Yu-Lin; Chen, Hsing-Yin
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 10.0533 ± 0.0005 Å
• b: 10.1641 ± 0.0006 Å
• c: 10.8552 ± 0.0006 Å
• α: 63.909 ± 0.002°
• β: 72.068 ± 0.002°
• γ: 64.666 ± 0.002°
• Cell volume: 890.53 ± 0.09 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0516
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for significantly intense reflections: 0.1046
• Weighted residual factors for all reflections included in the refinement: 0.1126
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No