Information card for entry 4038387

Structure parameters

• Formula: C15 H14 O4 S2
• Calculated formula: C15 H14 O4 S2
• Title of publication: CuBr₂-Mediated One-Pot Synthesis of Sulfonyl 9-Fluorenylidenes.
• Authors of publication: Chang, Meng-Yang; Tsai, Yu-Lin; Chen, Hsing-Yin
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 8.6178 ± 0.0007 Å
• b: 9.0183 ± 0.0007 Å
• c: 9.6399 ± 0.0008 Å
• α: 79.873 ± 0.004°
• β: 75.377 ± 0.004°
• γ: 85.646 ± 0.004°
• Cell volume: 713.24 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.036
• Residual factor for significantly intense reflections: 0.0321
• Weighted residual factors for significantly intense reflections: 0.0793
• Weighted residual factors for all reflections included in the refinement: 0.0824
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No