Information card for entry 4038398

Structure parameters

• Formula: C22 H19 Au Cl O P
• Calculated formula: C22 H19 Au Cl O P
• Title of publication: Concise Synthesis of Phospholene and Its P-Stereogenic Derivatives.
• Authors of publication: Hu, Wei; Li, Er-Qing; Duan, Zheng; Mathey, François
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 25.9881 ± 0.0004 Å
• b: 25.9881 ± 0.0004 Å
• c: 13.308 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8988 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 90
• Hermann-Mauguin space group symbol: P 4 21 2
• Hall space group symbol: P 4ab 2ab
• Residual factor for all reflections: 0.0476
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1155
• Weighted residual factors for all reflections included in the refinement: 0.12
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No