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Information card for entry 4038660
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Coordinates | 4038660.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C19 H47 P Si4 |
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Calculated formula | C19 H47 P Si4 |
Title of publication | Trialkylphosphines Having a Bulky Phosphacyclopentane Backbone: Structural and Redox Properties Depending on the Exocyclic Alkyl Groups and EPR Observation of a Persistent Trialkylphosphine Radical Cation. |
Authors of publication | Hirakawa, Fumiya; Nakagawa, Hiroshi; Honda, Shunya; Ishida, Shintaro; Iwamoto, Takeaki |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2020 |
a | 8.501 ± 0.002 Å |
b | 11.132 ± 0.003 Å |
c | 15.43 ± 0.004 Å |
α | 106.972 ± 0.002° |
β | 91.957 ± 0.003° |
γ | 109.448 ± 0.002° |
Cell volume | 1302.9 ± 0.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0351 |
Residual factor for significantly intense reflections | 0.0317 |
Weighted residual factors for significantly intense reflections | 0.0812 |
Weighted residual factors for all reflections included in the refinement | 0.0833 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4038660.html
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Users of the data should acknowledge the original authors of the
structural data.