Information card for entry 4038711
Formula
C37 H39 N O4 S
Calculated formula
C37 H39 N O4 S
Title of publication
Synthesis of 1,4-Dihydroquinolines and 4<i>H</i>-Chromenes via Organocatalytic Domino Aza/Oxa-Michael/1,6-Addition Reactions of <i>para</i>-Quinone Methides and Ynals.
Authors of publication
Wang, Junwei; Rong, Quanjin; Zhao, Lei; Pan, Xiang; Zhao, Lin; Zhao, Kun; Hu, Lihong
Journal of publication
The Journal of organic chemistry
Year of publication
2020
a
9.0613 ± 0.001 Å
b
17.674 ± 0.002 Å
c
20.106 ± 0.002 Å
α
90°
β
101.443 ± 0.005°
γ
90°
Cell volume
3156 ± 0.6 Å3
Cell temperature
190 ± 2 K
Ambient diffraction temperature
190 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.077
Residual factor for significantly intense reflections
0.0534
Weighted residual factors for significantly intense reflections
0.1333
Weighted residual factors for all reflections included in the refinement
0.1458
Goodness-of-fit parameter for all reflections included in the refinement
1.019
Diffraction radiation wavelength
1.34139 Å
Diffraction radiation type
GaKα
Has coordinates
Yes
Has disorder
No
Has Fobs
No
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https://www.crystallography.net/4038711.html