Information card for entry 4038810

Structure parameters

• Formula: C80 H132 Au2 Cl2 O P4
• Calculated formula: C80 H132 Au2 Cl2 O P4
• Title of publication: Selective Pd-Catalyzed Monoarylation of Small Primary Alkyl Amines through Backbone-Modification in Ylide-Functionalized Phosphines (YPhos).
• Authors of publication: Rodstein, Ilja; Prendes, Daniel Sowa; Wickert, Leon; Paaßen, Maurice; Gessner, Viktoria
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 10.22661 ± 0.00016 Å
• b: 10.50804 ± 0.00018 Å
• c: 18.1253 ± 0.0003 Å
• α: 86.2203 ± 0.0014°
• β: 86.1003 ± 0.0013°
• γ: 79.6142 ± 0.0014°
• Cell volume: 1908.57 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0225
• Residual factor for significantly intense reflections: 0.0217
• Weighted residual factors for significantly intense reflections: 0.0554
• Weighted residual factors for all reflections included in the refinement: 0.0558
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No