Information card for entry 4038836

Structure parameters

• Formula: C26 H24 N O P
• Calculated formula: C26 H24 N O P
• Title of publication: Synthesis of α-aminophosphonates via phosphonylation of an aryne-imine adduct.
• Authors of publication: Lim, Taehyun; Kim, Byeong Moon
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 18.889 ± 0.004 Å
• b: 11.865 ± 0.002 Å
• c: 19.04 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4267.2 ± 1.6 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1547
• Residual factor for significantly intense reflections: 0.0703
• Weighted residual factors for significantly intense reflections: 0.1833
• Weighted residual factors for all reflections included in the refinement: 0.2366
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No