Crystallography Open Database

Information card for entry 4038839

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Coordinates	4038839.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H14 N2
Calculated formula	C16 H14 N2
Title of publication	Palladium-catalyzed Monoarylation of Arylhydrazines with Aryl Tosylates.
Authors of publication	Huang, Yange; Choy, Pui Ying; Wang, Junya; Tse, Man Kin; Sun, Raymond Wai-Yin; Chan, Albert Sun Chi; Kwong, Fuk Yee
Journal of publication	The Journal of organic chemistry
Year of publication	2020
a	23.2393 ± 0.0013 Å
b	7.5636 ± 0.0004 Å
c	7.3759 ± 0.0004 Å
α	90°
β	100.902 ± 0.003°
γ	90°
Cell volume	1273.08 ± 0.12 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	3
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0494
Residual factor for significantly intense reflections	0.0391
Weighted residual factors for significantly intense reflections	0.1052
Weighted residual factors for all reflections included in the refinement	0.1167
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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