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Information card for entry 4038871
Preview
Coordinates | 4038871.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C42 H58 B2 F8 N2 Ni P4 |
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Calculated formula | C42 H58 B2 F8 N2 Ni P4 |
Title of publication | Dynamic covalent chemistry approach toward 18-membered P<sub>4</sub>N<sub>2</sub> macrocycles and their nickel(II) complexes. |
Authors of publication | Musina, Elvira I.; Wittmann, Tatiana I.; Musin, Lenar; Balueva, Anna S.; Shpagina, Alena S.; Litvinov, Igor A.; Lönnecke, Peter; Hey-Hawkins, Evamarie; Karasik, Andrey A.; Sinyashin, Oleg G. |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2020 |
a | 13.1558 ± 0.0002 Å |
b | 21.3869 ± 0.0003 Å |
c | 16.3943 ± 0.0003 Å |
α | 90° |
β | 108.413 ± 0.002° |
γ | 90° |
Cell volume | 4376.58 ± 0.13 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0737 |
Residual factor for significantly intense reflections | 0.0449 |
Weighted residual factors for significantly intense reflections | 0.0906 |
Weighted residual factors for all reflections included in the refinement | 0.1017 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4038871.html
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