Crystallography Open Database

Information card for entry 4038876

Preview

Coordinates	4038876.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H27 N O4
Calculated formula	C24 H27 N O4
Title of publication	Construction of the Erythrinane Core Skeleton via Asymmetric Catalytic Cascade Reaction of Tertiary Enamides.
Authors of publication	Zhen, Li; Tong, Shuo; Zhu, Jieping; Wang, Mei-Xiang
Journal of publication	The Journal of organic chemistry
Year of publication	2020
Journal volume	85
Journal issue	20
Pages of publication	13211 - 13219
a	6.0637 ± 0.0001 Å
b	16.8612 ± 0.0002 Å
c	19.9302 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	2037.69 ± 0.05 Å³
Cell temperature	169.99 ± 0.11 K
Ambient diffraction temperature	169.99 ± 0.11 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0441
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.1055
Weighted residual factors for all reflections included in the refinement	0.1116
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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