Information card for entry 4060018

Structure parameters

• Formula: C14 H15 N O5 P2 W
• Calculated formula: C14 H15 N O5 P2 W
• Title of publication: Design, Synthesis, and Chemistry of Sterically Nondemanding Primary Bisphosphines^1^
• Authors of publication: Pillarsetty, Nagavarakishore; Raghuraman, Kannan; Barnes, Charles L.; Katti, Kattesh V.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2005
• Journal volume: 127
• Journal issue: 1
• Pages of publication: 331 - 336
• a: 8.6521 ± 0.0008 Å
• b: 17.2931 ± 0.0015 Å
• c: 23.187 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3469.3 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0756
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.0898
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No