Information card for entry 4060293

Structure parameters

• Formula: C24.5 H34 Cl Os P
• Calculated formula: C24.5 H23 Cl Os P
• Title of publication: Ene-Type Reactions between an α-Alkenylphosphine and Terminal Alkynes Promoted by Osmium-Cyclopentadienyl Fragments
• Authors of publication: Baya, Miguel; Buil, María L.; Esteruelas, Miguel A.; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 9
• Pages of publication: 2030 - 2038
• a: 7.6298 ± 0.0005 Å
• b: 11.3416 ± 0.0007 Å
• c: 14.0086 ± 0.0008 Å
• α: 103.785 ± 0.001°
• β: 95.97 ± 0.001°
• γ: 91.487 ± 0.001°
• Cell volume: 1169.3 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0285
• Weighted residual factors for significantly intense reflections: 0.0627
• Weighted residual factors for all reflections included in the refinement: 0.0636
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No