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Information card for entry 4060497
Preview
Coordinates | 4060497.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C48 H54 Cl7 F6 P2 Ru Sb |
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Calculated formula | C46 H52 Cl F6.014 P2 Ru Sb |
Title of publication | Ruthenium Complexes of Six-Electron-Donor NUPHOS-Type Diphosphines: Highly Selective Catalysts for the Hydrocarboxylation of Terminal Alkynes |
Authors of publication | Doherty, Simon; Knight, Julian G.; Rath, Rakesh K.; Clegg, William; Harrington, Ross W.; Newman, Colin R.; Campbell, Robert; Amin, Hiren |
Journal of publication | Organometallics |
Year of publication | 2005 |
Journal volume | 24 |
Journal issue | 11 |
Pages of publication | 2633 - 2644 |
a | 10.1035 ± 0.0005 Å |
b | 28.61 ± 0.005 Å |
c | 18.303 ± 0.005 Å |
α | 90° |
β | 97.25 ± 0.006° |
γ | 90° |
Cell volume | 5248.4 ± 1.6 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0768 |
Residual factor for significantly intense reflections | 0.0569 |
Weighted residual factors for significantly intense reflections | 0.1509 |
Weighted residual factors for all reflections included in the refinement | 0.1599 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.108 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4060497.html
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