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Information card for entry 4060499
Preview
Coordinates | 4060499.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C96 H92 Cl10 F12 P4 Ru2 Sb2 |
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Calculated formula | C96 H92 Cl10 F12 P4 Ru2 Sb2 |
Title of publication | Ruthenium Complexes of Six-Electron-Donor NUPHOS-Type Diphosphines: Highly Selective Catalysts for the Hydrocarboxylation of Terminal Alkynes |
Authors of publication | Doherty, Simon; Knight, Julian G.; Rath, Rakesh K.; Clegg, William; Harrington, Ross W.; Newman, Colin R.; Campbell, Robert; Amin, Hiren |
Journal of publication | Organometallics |
Year of publication | 2005 |
Journal volume | 24 |
Journal issue | 11 |
Pages of publication | 2633 - 2644 |
a | 14.7948 ± 0.0013 Å |
b | 17.8716 ± 0.0015 Å |
c | 19.9255 ± 0.0017 Å |
α | 97.429 ± 0.001° |
β | 94.401 ± 0.002° |
γ | 111.458 ± 0.001° |
Cell volume | 4818 ± 0.7 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.125 |
Residual factor for significantly intense reflections | 0.0714 |
Weighted residual factors for significantly intense reflections | 0.1686 |
Weighted residual factors for all reflections included in the refinement | 0.2019 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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