Information card for entry 4060817

Structure parameters

• Formula: C30 H48 Cl Ir3 S4
• Calculated formula: C30 H48 Cl Ir3 S4
• Title of publication: Synthesis of a New Tetrakis(hydrosulfido) Diiridium Complex and Its Conversion into Homo- and Heterometallic Sulfido-Hydrosulfido Clusters
• Authors of publication: Takagi, Fusao; Seino, Hidetake; Mizobe, Yasushi; Hidai, Masanobu
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 4
• Pages of publication: 694 - 699
• a: 9.894 ± 0.002 Å
• b: 19.736 ± 0.003 Å
• c: 18.098 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3533 ± 1 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 5
• Space group number: 57
• Hermann-Mauguin space group symbol: P b c m
• Hall space group symbol: -P 2c 2b
• Residual factor for all reflections: 0.0327
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.034
• Weighted residual factors for all reflections included in the refinement: 0.034
• Goodness-of-fit parameter for all reflections included in the refinement: 1.298
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No