Information card for entry 4063223

Structure parameters

• Formula: ?
• Calculated formula: C40 H64 Cl4 Ir4 S4
• Title of publication: The Hydrosulfido-Bridged Diiridium and Dirhodium Complexes [Cp*MCl(μ2-SH)2MCp*Cl] (M =Ir, Rh; Cp* =μ5-C5Me5) as Versatile Precursors for Tri- and Tetranuclear Sulfido Clusters
• Authors of publication: Zhen Tang; Yasuo Nomura; Youichi Ishii; Yasushi Mizobe; Masanobu Hidai
• Journal of publication: Organometallics
• Year of publication: 1997
• Journal volume: 16
• Journal issue: 2
• Pages of publication: 151 - 154
• a: 8.519 ± 0.0006 Å
• b: 9.2733 ± 0.0007 Å
• c: 15.679 ± 0.0007 Å
• α: 90°
• β: 104.06 ± 0.005°
• γ: 90°
• Cell volume: 1201.5 ± 0.1 ų
• Cell temperature: 20 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.024
• Goodness-of-fit parameter for significantly intense reflections: 2.18
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No