Information card for entry 4063227

Structure parameters

• Formula: C560 H712 Cl16 O64 P16 Rh8
• Calculated formula: C560 H712 Cl16 O64 P16 Rh8
• Title of publication: Bulky Diphosphite-Modified Rhodium Catalysts: Hydroformylation and Characterization
• Authors of publication: Annemiek van Rooy; Paul C. J. Kamer; Piet W. N. M. van Leeuwen; Kees Goubitz; Jan Fraanje; Nora Veldman; Anthony L. Spek
• Journal of publication: Organometallics
• Year of publication: 1996
• Journal volume: 15
• Journal issue: 2
• Pages of publication: 835 - 847
• a: 40.632 ± 0.006 Å
• b: 13.943 ± 0.003 Å
• c: 23.645 ± 0.005 Å
• α: 90°
• β: 92.42 ± 0.015°
• γ: 90°
• Cell volume: 13383.7 ± 4.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1877
• Residual factor for significantly intense reflections: 0.0815
• Weighted residual factors for all reflections: 0.1643
• Weighted residual factors for significantly intense reflections: 0.1374
• Goodness-of-fit parameter for all reflections: 0.935
• Goodness-of-fit parameter for significantly intense reflections: 1.169
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No