Crystallography Open Database

Information card for entry 4063246

Preview

Coordinates	4063246.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H38 F6 Fe P4
Calculated formula	C24 H38 F6 Fe P4
Title of publication	Synthesis and Characterization of Iron(II) Complexes of 10- and 11-Membered Triphosphamacrocycles
Authors of publication	Andrew R. Battle; Peter G. Edwards; Robert Haigh; David E. Hibbs; Dongmei Li; Sam M. Liddiard; Paul D. Newman
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Pages of publication	377 - 386
a	42.467 ± 0.006 Å
b	42.467 ± 0.006 Å
c	9.69 ± 0.002 Å
α	90°
β	90°
γ	120°
Cell volume	15134 ± 4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.1045
Residual factor for significantly intense reflections	0.0771
Weighted residual factors for significantly intense reflections	0.2155
Weighted residual factors for all reflections included in the refinement	0.2286
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4063246.html