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Information card for entry 4063267
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 4063267.cif |
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Original paper (by DOI) | HTML |
Formula | C48 H50 B N3 Pd |
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Calculated formula | C48 H50 B N3 Pd |
Title of publication | Phosphine- and Pyridine-Functionalized N-Heterocyclic Carbene Methyl and Allyl Complexes of Palladium. Unexpected Regiospecificity of the Protonation Reaction of the Dimethyl Complexes |
Authors of publication | Andreas A. Danopoulos; Nikolaos Tsoureas; Stuart A. Macgregor; Christopher Smith |
Journal of publication | Organometallics |
Year of publication | 2007 |
Journal volume | 26 |
Pages of publication | 253 - 263 |
a | 13.149 ± 0.002 Å |
b | 14.181 ± 0.002 Å |
c | 15.6998 ± 0.0017 Å |
α | 115.11 ± 0.012° |
β | 90.856 ± 0.013° |
γ | 114.148 ± 0.016° |
Cell volume | 2355 ± 0.8 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0989 |
Residual factor for significantly intense reflections | 0.068 |
Weighted residual factors for significantly intense reflections | 0.1597 |
Weighted residual factors for all reflections included in the refinement | 0.1735 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4063267.html
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