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Information card for entry 4063269
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Coordinates | 4063269.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C59 H45 B F24 N4 Pd |
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Calculated formula | C59 H45 B F24 N4 Pd |
Title of publication | Phosphine- and Pyridine-Functionalized N-Heterocyclic Carbene Methyl and Allyl Complexes of Palladium. Unexpected Regiospecificity of the Protonation Reaction of the Dimethyl Complexes |
Authors of publication | Andreas A. Danopoulos; Nikolaos Tsoureas; Stuart A. Macgregor; Christopher Smith |
Journal of publication | Organometallics |
Year of publication | 2007 |
Journal volume | 26 |
Pages of publication | 253 - 263 |
a | 24.5559 ± 0.0008 Å |
b | 19.7453 ± 0.0007 Å |
c | 25.285 ± 0.008 Å |
α | 90° |
β | 97.34 ± 0.001° |
γ | 90° |
Cell volume | 12159 ± 4 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1526 |
Residual factor for significantly intense reflections | 0.0786 |
Weighted residual factors for significantly intense reflections | 0.1731 |
Weighted residual factors for all reflections included in the refinement | 0.2053 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4063269.html
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structural data.