Information card for entry 4063288

Structure parameters

• Formula: C51 H48 Cl2 Fe2 O8 Ru2 Si
• Calculated formula: C51 H47 Cl2 Fe2 O8 Ru2 Si
• Title of publication: C-C Coupling of a Permetalated Ethene, (μ4-C=C)Ru2(FeCp*)2(CO)10, with Alkynes, and Isolation of a Labile MeCN Adduct, (μ4-C\δb C)Ru2(FeCp*)2(CO)8(NCMe)2
• Authors of publication: Gou Higashihara; Masako Terada; Akiko Inagaki; Munetaka Akita
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Pages of publication: 439 - 444
• a: 17.875 ± 0.002 Å
• b: 19.581 ± 0.002 Å
• c: 14.3792 ± 0.0008 Å
• α: 101.1 ± 0.005°
• β: 97.559 ± 0.004°
• γ: 85.12 ± 0.002°
• Cell volume: 4886.7 ± 0.7 ų
• Cell temperature: 213 K
• Ambient diffraction temperature: 213 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0837
• Weighted residual factors for all reflections included in the refinement: 0.2055
• Goodness-of-fit parameter for all reflections included in the refinement: 0.86
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No