Information card for entry 4063305

Structure parameters

• Common name: 1R(S),2S(R)-1,2-Bis(trichlorosilyl)-1,2-diphenylethane
• Formula: C7 H6 Cl3 Si
• Calculated formula: C7 H6 Cl3 Si
• Title of publication: Double Silylation of Olefin with HSiCl3 in the Presence of Bu4PCl. New Synthetic Method for α,β-Bis(trichlorosilyl)alkanes
• Authors of publication: Seung-Hyun Kang; Joon Soo Han; Weon Cheol Lim; Il Nam Jung; Myong Euy Lee; Bok Ryul Yoo
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 2
• Pages of publication: 318 - 319
• a: 6.4332 ± 0.0015 Å
• b: 8.6245 ± 0.0015 Å
• c: 9.584 ± 0.002 Å
• α: 79.85 ± 0.02°
• β: 71.86 ± 0.02°
• γ: 68.32 ± 0.02°
• Cell volume: 468.47 ± 0.17 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0667
• Weighted residual factors for significantly intense reflections: 0.1794
• Weighted residual factors for all reflections included in the refinement: 0.1798
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No