Information card for entry 4063352

Structure parameters

• Formula: C74 H59 B F24 P3 Ru
• Calculated formula: C74 H52 B F24 P3 Ru
• Title of publication: Reversibility of Disubstituted Vinylidene - Internal Alkyne Isomerization at Cationic Ruthenium and Iron Complexes
• Authors of publication: Mutoh, Yuichiro; Imai, Kohei; Kimura, Yusuke; Ikeda, Yousuke; Ishii, Youichi
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 2
• Pages of publication: 204 - 207
• a: 12.691 ± 0.003 Å
• b: 15.192 ± 0.003 Å
• c: 19.27 ± 0.004 Å
• α: 69.846 ± 0.004°
• β: 84.795 ± 0.007°
• γ: 82.398 ± 0.006°
• Cell volume: 3453.1 ± 1.3 ų
• Cell temperature: 123.1 K
• Ambient diffraction temperature: 123.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0647
• Weighted residual factors for all reflections included in the refinement: 0.1617
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No