Palladium Complexes with Carbene and Phosphine Ligands: Synthesis, Structural Characterization, and Direct Arylation Reactions between Aryl Halides and Alkynes
Authors of publication
Chan, Kai-Ting; Tsai, Yi-Hua; Lin, Wu-Shien; Wu, Jia-Rong; Chen, Shih-Jung; Liao, Fu-Xing; Hu, Ching-Han; Lee, Hon Man
Journal of publication
Organometallics
Year of publication
2010
Journal volume
29
Journal issue
2
Pages of publication
463 - 472
a
23.555 ± 0.015 Å
b
7.215 ± 0.005 Å
c
19.145 ± 0.013 Å
α
90°
β
119.881 ± 0.011°
γ
90°
Cell volume
2821 ± 3 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
2
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0747
Residual factor for significantly intense reflections
0.0506
Weighted residual factors for significantly intense reflections
0.1579
Weighted residual factors for all reflections included in the refinement
0.1766
Goodness-of-fit parameter for all reflections included in the refinement
