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Information card for entry 4063495
Preview
Coordinates | 4063495.cif |
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Original paper (by DOI) | HTML |
Formula | C26 H44 O4 Si2 |
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Calculated formula | C26 H44 O4 Si2 |
SMILES | [Si](C=C=C=C([Si](C)(C)C(C)(C)C)C(O)c1cc(OC)c(OC)c(OC)c1)(C)(C)C(C)(C)C |
Title of publication | Highly Stereoselective Synthesis of Trisubstituted cis-[3]Cumulenols from Alkynylated Oxatitanacycles in the Presence of Lewis acids |
Authors of publication | Chen, Jingjin; Liu, Yuanhong |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 2 |
Pages of publication | 505 - 508 |
a | 7.9041 ± 0.0008 Å |
b | 12.4809 ± 0.0013 Å |
c | 16.3912 ± 0.0016 Å |
α | 111.863 ± 0.002° |
β | 90.997 ± 0.002° |
γ | 99.96 ± 0.002° |
Cell volume | 1472.1 ± 0.3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1111 |
Residual factor for significantly intense reflections | 0.0707 |
Weighted residual factors for significantly intense reflections | 0.1802 |
Weighted residual factors for all reflections included in the refinement | 0.2025 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.956 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4063495.html
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