Information card for entry 4063499

Structure parameters

• Formula: C25 H33 Cl N P Ru
• Calculated formula: C25 H33 Cl N P Ru
• SMILES: [Ru]12345(Cl)([P](C[C@@H]([NH2]1)C)(c1ccccc1)c1ccccc1)[c]1([c]2([c]3([c]4([c]51C)C)C)C)C
• Title of publication: A Convenient Method for the Synthesis of Protic 2-(Tertiary phosphino)-1-amines and Their Cp*RuCl Complexes
• Authors of publication: Ito, Masato; Osaku, Akihide; Kobayashi, Chika; Shiibashi, Akira; Ikariya, Takao
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 2
• Pages of publication: 390 - 393
• a: 11.48 ± 0.002 Å
• b: 12.029 ± 0.002 Å
• c: 17.813 ± 0.004 Å
• α: 90°
• β: 94.975 ± 0.002°
• γ: 90°
• Cell volume: 2450.6 ± 0.8 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for significantly intense reflections: 0.028
• Weighted residual factors for all reflections included in the refinement: 0.083
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No