Information card for entry 4063791

Structure parameters

• Formula: C64 H55 B F24 P Rh
• Calculated formula: C64 H55 B F24 P Rh
• Title of publication: Synthesis, Characterization, and Reactivity of Arene-Stabilized Rhodium Complexes
• Authors of publication: O’Connor, Abby R.; Kaminsky, Werner; Heinekey, D. Michael; Goldberg, Karen I.
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 8
• Pages of publication: 2105
• a: 36.1427 ± 0.0011 Å
• b: 13.1127 ± 0.0004 Å
• c: 25.4551 ± 0.0008 Å
• α: 90°
• β: 97.883 ± 0.002°
• γ: 90°
• Cell volume: 11949.9 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0923
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1024
• Weighted residual factors for all reflections included in the refinement: 0.1178
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No