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Information card for entry 4063806
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Coordinates | 4063806.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | 1-(2,2,6,6-tetramethylpiperidinium)-2-[tris(pentafluorophenyl)boryl]ethane |
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Formula | C29 H21 B F15 N |
Calculated formula | C29 H21 B F15 N |
Title of publication | Heterolytic Cleavage of H2by Frustrated B/N Lewis Pairs |
Authors of publication | Jiang, Chunfang; Blacque, Olivier; Fox, Thomas; Berke, Heinz |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 8 |
Pages of publication | 2117 |
a | 23.0895 ± 0.0003 Å |
b | 11.0393 ± 0.0002 Å |
c | 21.5309 ± 0.0003 Å |
α | 90° |
β | 90.593 ± 0.001° |
γ | 90° |
Cell volume | 5487.76 ± 0.14 Å3 |
Cell temperature | 183 ± 2 K |
Ambient diffraction temperature | 183 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.063 |
Residual factor for significantly intense reflections | 0.046 |
Weighted residual factors for significantly intense reflections | 0.1254 |
Weighted residual factors for all reflections included in the refinement | 0.1314 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.105 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4063806.html
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