Information card for entry 4063838

Structure parameters

• Formula: C111 H104 P8 Pt4 Si
• Calculated formula: C107.5 H98.5 P8 Pt4 Si
• Title of publication: Polyhedral and Spiro Platinum−Silyl Clusters Bearing Phosphine Ligands
• Authors of publication: Arii, Hidekazu; Takahashi, Makiko; Nanjo, Masato; Mochida, Kunio
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 4
• Pages of publication: 917
• a: 18.399 ± 0.0014 Å
• b: 14.3441 ± 0.0011 Å
• c: 19.3468 ± 0.0014 Å
• α: 90°
• β: 93.294 ± 0.001°
• γ: 90°
• Cell volume: 5097.5 ± 0.7 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.03
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.0842
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No