Information card for entry 4063857

Structure parameters

• Formula: C28 H54 N3 O Si4 Yb
• Calculated formula: C28 H54 N3 O Si4 Yb
• SMILES: [Yb]([O]1CCCC1)(N(c1ccccc1)c1ccccc1)(N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Fast Synthesis of Hydrazine and Azo Derivatives by Oxidation of Rare-Earth-Metal−Nitrogen Bonds
• Authors of publication: Zhang, Lijun; Xia, Jing; Li, Qinghai; Li, Xihong; Wang, Shaowu
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 3
• Pages of publication: 375
• a: 9.3442 ± 0.0011 Å
• b: 10.8748 ± 0.0013 Å
• c: 19.243 ± 0.002 Å
• α: 100.656 ± 0.001°
• β: 100.726 ± 0.001°
• γ: 102.265 ± 0.001°
• Cell volume: 1825.4 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0289
• Residual factor for significantly intense reflections: 0.0236
• Weighted residual factors for significantly intense reflections: 0.0618
• Weighted residual factors for all reflections included in the refinement: 0.0642
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No