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Information card for entry 4063872
Preview
Coordinates | 4063872.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C116.25 H107.5 Cl6.5 F3 N2 O7 Os2 P8 Rh2 S |
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Calculated formula | C116.25 H107.5 Cl6.5 F3 N2 O7 Os2 P8 Rh2 S |
Title of publication | Ethylene Substitution in a Bis-Ethylene Complex of Rh/Os and Unusual Brønsted−Lowry Basicity of an N-Heterocyclic Carbene |
Authors of publication | Wells, Kyle D.; Ferguson, Michael J.; McDonald, Robert; Cowie, Martin |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 4 |
Pages of publication | 815 |
a | 15.8631 ± 0.0009 Å |
b | 19.6777 ± 0.0011 Å |
c | 21.6108 ± 0.0012 Å |
α | 96.9515 ± 0.0007° |
β | 106.386 ± 0.0007° |
γ | 111.141 ± 0.0006° |
Cell volume | 5846.2 ± 0.6 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 10 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0367 |
Residual factor for significantly intense reflections | 0.0278 |
Weighted residual factors for significantly intense reflections | 0.0781 |
Weighted residual factors for all reflections included in the refinement | 0.0849 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4063872.html
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