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Information card for entry 4063878
Preview
Coordinates | 4063878.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C58.25 H55.5 Cl2.5 F3 O6 Os P5 Rh S |
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Calculated formula | C58.25 H55.5 Cl2.5 F3 O6 Os P5 Rh S |
Title of publication | Influences of N-Heterocyclic Carbene and PMe3Ligands on the Tautomerism between Methylene/Hydride and Bridging Methyl Complexes of Rh/Os and Unusual Examples of Ligand Deprotonation by the NHC Group |
Authors of publication | Wells, Kyle D.; McDonald, Robert; Ferguson, Michael J.; Cowie, Martin |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 10 |
Pages of publication | 2654 |
a | 12.7428 ± 0.0017 Å |
b | 15.891 ± 0.002 Å |
c | 17.468 ± 0.002 Å |
α | 90.12 ± 0.0018° |
β | 106.618 ± 0.0018° |
γ | 108.115 ± 0.0017° |
Cell volume | 3205.3 ± 0.7 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 9 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0672 |
Residual factor for significantly intense reflections | 0.0513 |
Weighted residual factors for significantly intense reflections | 0.1392 |
Weighted residual factors for all reflections included in the refinement | 0.149 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.053 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4063878.html
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