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Information card for entry 4063900
Preview
Coordinates | 4063900.cif |
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Original paper (by DOI) | HTML |
Chemical name | [bis[N-2-(dimethylstibanyl)benzyl]methanamine]- bis(dicarbonyl(cyclopentadienyl)iron(II)) tetrafluoroborate dichloromethane solvate |
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Formula | C33.5 H38 B2 Cl F8 Fe2 N O4 Sb2 |
Calculated formula | C33.5 H38 B2 Cl F8 Fe2 N O4 Sb2 |
Title of publication | Hybrid Dibismuthines and Distibines: Preparation and Properties of Antimony and Bismuth Oxygen, Sulfur, and Nitrogen Donor Ligands |
Authors of publication | Benjamin, Sophie L.; Karagiannidis, Louise; Levason, William; Reid, Gillian; Rogers, Michael C. |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 4 |
Pages of publication | 895 |
a | 10.5977 ± 0.001 Å |
b | 11.799 ± 0.002 Å |
c | 16.732 ± 0.003 Å |
α | 78.332 ± 0.006° |
β | 86.814 ± 0.008° |
γ | 85.261 ± 0.008° |
Cell volume | 2040.3 ± 0.5 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 9 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1141 |
Residual factor for significantly intense reflections | 0.0843 |
Weighted residual factors for significantly intense reflections | 0.169 |
Weighted residual factors for all reflections included in the refinement | 0.1881 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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