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Information card for entry 4063953
Preview
Coordinates | 4063953.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H48 Os P2 |
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Calculated formula | C32 H48 Os P2 |
SMILES | [c]12([p]3[Os]4567891([c]3([cH]4[cH]26)C1CCCCC1)[c]1([cH]5[cH]7[c]8([p]91)C1CCCCC1)C1CCCCC1)C1CCCCC1 |
Title of publication | Preparation of Osmium η5-Phospholide Complexes and Their Reactions with Acyl Electrophiles: C═O Bond Cleavage and C−C Bond Formation within the Metal Coordination Sphere |
Authors of publication | Ogasawara, Masamichi; Shintani, Minoru; Watanabe, Susumu; Sakamoto, Takeshi; Nakajima, Kiyohiko; Takahashi, Tamotsu |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 6 |
Pages of publication | 1487 |
a | 6.1365 ± 0.0001 Å |
b | 9.8469 ± 0.0002 Å |
c | 13.4415 ± 0.0003 Å |
α | 72.2309 ± 0.0009° |
β | 79.1741 ± 0.001° |
γ | 75.0332 ± 0.001° |
Cell volume | 741.96 ± 0.03 Å3 |
Cell temperature | 298.1 K |
Ambient diffraction temperature | 298 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for significantly intense reflections | 0.0199 |
Weighted residual factors for all reflections included in the refinement | 0.0418 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.067 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4063953.html
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