Information card for entry 4063971

Structure parameters

• Formula: C64 H84 N8 O2 Si2
• Calculated formula: C64 H84 N8 O2 Si2
• Title of publication: Synthesis of a Lewis Base Stabilized Dimer of N-Substituted Hydrosila Hydrazone and a Silaaziridine
• Authors of publication: Sarish, Sankaranarayana Pillai; Jana, Anukul; Roesky, Herbert W.; Samuel, Prinson P.; Andrade, Carlos E. Abad; Dittrich, Birger; Schulzke, Carola
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 4
• Pages of publication: 912
• a: 12.7543 ± 0.0003 Å
• b: 18.2098 ± 0.0004 Å
• c: 13.9106 ± 0.0003 Å
• α: 90°
• β: 113.129 ± 0.0007°
• γ: 90°
• Cell volume: 2971.11 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0959
• Weighted residual factors for all reflections included in the refinement: 0.096
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No