Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4064007
Preview
Coordinates | 4064007.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39.5 H50 Cl2 N2 O0.5 P Pd Pt |
---|---|
Calculated formula | C39.5 H50 Cl2 N2 O0.5 P Pd Pt |
Title of publication | Asymmetric Synthesis of P-Stereogenic Homo- and Heterobimetallic Complexes via Selective Monoinsertion of Dialkynylphosphine into the Pd−C Bond of a Palladacycle |
Authors of publication | Chen, Shuli; Pullarkat, Sumod A.; Li, Yongxin; Leung, Pak-Hing |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 6 |
Pages of publication | 1530 |
a | 11.9361 ± 0.0007 Å |
b | 15.1004 ± 0.0009 Å |
c | 12.6209 ± 0.0008 Å |
α | 90° |
β | 97.846 ± 0.002° |
γ | 90° |
Cell volume | 2253.5 ± 0.2 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 8 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0908 |
Residual factor for significantly intense reflections | 0.0549 |
Weighted residual factors for significantly intense reflections | 0.1435 |
Weighted residual factors for all reflections included in the refinement | 0.1816 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.087 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4064007.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.